奥贝胆酸杂质 结构确证图谱

中文名称

英文名称

CAS号

奥贝胆酸标准品

Obeticholic Acid

459789-99-2

奥贝胆酸杂质1

(R)-4-((3R,5S,6R,7S,8S,9S,10S,13R,14S,17R)-6-ethyl-3,7-dihydroxy-10,13-dimethylhexadecahydro-1H-cyclopenta[a]phenanthren-17-yl)pentanoic acid

865244-30-0

奥贝胆酸杂质2

(R)-4-((3R,5S,6R,8S,9S,10S,13R,14S,17R)-6-ethyl-3-hydroxy-10,13-dimethyl-7-oxohexadecahydro-1H-cyclopenta[a]phenanthren-17-yl)pentanoic acid

915038-26-5

奥贝胆酸杂质3

(R)-4-((3R,5S,6S,7R,8S,9S,10S,13R,14S,17R)-6-ethyl-3,7-dihydroxy-10,13-dimethylhexadecahydro-1H-cyclopenta[a]phenanthren-17-yl)pentanoic acid

915038-27-6

奥贝胆酸杂质4

(R)-4-((3R,5R,7S,8S,9S,10R,13R,14S,17R)-6-ethylidene-3,7-dihydroxy-10,13-dimethylhexadecahydro-1H-cyclopenta[a]phenanthren-17-yl)pentanoic acid

奥贝胆酸杂质5

(R)-4-((3R,5S,7R,8R,9S,10S,13R,14S,17R)-3,7-dihydroxy-10,13-dimethylhexadecahydro-1H-cyclopenta[a]phenanthren-17-yl)pentanoic acid

474-25-9

奥贝胆酸杂质6

(R)-4-((3R,5S,6R,7R,8S,9S,10S,13R,14S,17R)-6-ethyl-3-((((R)-4-((3R,5S,6R,7R,8S,9S,10S,13R,14S,17R)-6-ethyl-3,7-dihydroxy-10,13-dimethylhexadecahydro-1H-cyclopenta[a]phenanthren-17-yl)pentanoyl)oxy)methyl)-7-hydroxy-10,13-dimethylhexadecahydro-1H-cyclopenta[a]phenanthren-17-yl)pentanoic acid

奥贝胆酸杂质7

(R)-4-((3R,5S,6S,7S,8S,9S,10S,13R,14S,17R)-6-ethyl-3,7-dihydroxy-10,13-dimethylhexadecahydro-1H-cyclopenta[a]phenanthren-17-yl)pentanoic acid

1708092-13-0

奥贝胆酸杂质8

(3R,5S,6R,7R,8S,9S,10S,13R,14S,17R)-6-ethyl-17-((R)-5-hydroxypentan-2-yl)-10,13-dimethylhexadecahydro-1H-cyclopenta[a]phenanthrene-3,7-diol

1537866-49-1

奥贝胆酸杂质9

(R)-4-((3R,5S,8R,9S,10S,13R,14S,17R)-3-hydroxy-10,13-dimethyl-7-oxohexadecahydro-1H-cyclopenta[a]phenanthren-17-yl)pentanoic acid

4651-67-6

奥贝胆酸杂质10

(R)-methyl 4-((3R,5S,8R,9S,10S,13R,14S,17R)-3-hydroxy-10,13-dimethyl-7-oxohexadecahydro-1H-cyclopenta[a]phenanthren-17-yl)pentanoate

10538-59-7

奥贝胆酸杂质11

(R)-methyl 4-((3R,5S,6R,8S,9S,10S,13R,14S,17R)-6-ethyl-3-hydroxy-10,13-dimethyl-7-oxohexadecahydro-1H-cyclopenta[a]phenanthren-17-yl)pentanoate

奥贝胆酸杂质12

(R)-4-((3R,5R,8S,9S,10R,13R,14S,17R)-6-ethylidene-3-hydroxy-10,13-dimethyl-7-oxohexadecahydro-1H-cyclopenta[a]phenanthren-17-yl)pentanoic acid

915038-24-3

奥贝胆酸杂质13

(R)-4-((3R,5S,6S,8S,9S,10S,13R,14S,17R)-6-ethyl-3-hydroxy-10,13-dimethyl-7-oxohexadecahydro-1H-cyclopenta[a]phenanthren-17-yl)pentanoic acid

奥贝胆酸杂质14

(4R)-4-((3R,5S,6R,7R,9S,10S,13R,14S,17R)-6-ethyl-3-(((R)-4-((3R,5S,6R,7R,8S,9S,10S,13R,14S,17R)-6-ethyl-3,7-dihydroxy-10,13-dimethylhexadecahydro-1H-cyclopenta[a]phenanthren-17-yl)pentanoyl)oxy)-7-hydroxy-10,13-dimethylhexadecahydro-1H-cyclopenta[a]phenanthren-17-yl)pentanoic acid

奥贝胆酸杂质15

(R)-4-((3R,5R,7S,8S,9S,10R,13R,14S,17R,E)-6-ethylidene-3,7-dihydroxy-10,13-dimethylhexadecahydro-1H-cyclopenta[a]phenanthren-17-yl)pentanoic acid

奥贝胆酸杂质16

(R)-4-((5S,8R,9S,10S,13R,14S,17R)-10,13-dimethyl-3,7-dioxohexadecahydro-1H-cyclopenta[a]phenanthren-17-yl)pentanoic acid

DLM-7731-1  

PHENYL ISOCYANATE (PHENYL-D5, 98%)

CLM-8389-0.1  

EICOSAPENTAENOIC ACID (U-13C20, 98%+)

PCB-36  

3,3',5-TRICB UNLABELED 35 UG/ML IN ISOOCTANE

H-041  

(+/-)-11-HYDROXY-DELTA-9-THC (D3, 98%) 100 UG/ML IN METHANOL

DLM-324-0.1  

5,5-DIPHENYLHYDANTOIN (DIPHENYL-D10, 98%)

PCB-8  

2,4'-DICB UNLABELED 35 UG/ML IN ISOOCTANE

DLM-2611-PK  

CHOLIC ACID (2,2,4,4-D4, 98%)

EBC-1741  

2,3-DIBROMO-7,8-DCDD UNLABELED

CDNLM-4282-0.1  

L-ISOLEUCINE (13C6, 95-97%; 15N, 96-99%; 2,3-D2, 97%+)

DLM-1626-PK  

PROPENE (3,3,3-D3, 98%)

MF-SPIRULINA-N  

MouseExpress (15N, 98%) MOUSE FEED PREPARED WITH SPIRULINA (U-15N, 98%+)

NLM-4266-25  

CYTIDINE 5'-TRIPHOSPHATE, LITHIUM SALT (15N3, 96-98%) 90-95% PURE

ULM-8202-0  

L-VALINE UNLABELED

DLM-53-5  

ACETONITRILE-D3 "*" (D, 99.96%)

CNLM-4358-H  

L-METHIONINE-N-FMOC (13C5, 99%; 15N, 99%)

CNLM-281-H-MPT  

L-LEUCINE (13C6, 99%;15N, 99%) MICROBIOLOG/PYROGEN TEST

NLM-2036-PK  

L-SERINE (15N, 98%)

DLM-8863-PK  

CORTISONE (1,2-D2, 98%)

NLM-467-PK  

AMMONIUM CHLORIDE (15N, 99%)

CLM-1578-MPT-PK  

SODIUM L-LACTATE 20% W/W IN H2O (3-13C, 98%) MICROBIOLOGICAL/PYROGEN TESTED

CLM-1014-PK  

FLUOROMETHANE (13C, 99%)

JR-F04-25  

1,2,3,8-TETRACDF UNLABELED ~25 NG/ML IN NONANE

DLM-1216-PK  

D-XYLOSE (2-D, 98%)

ECB-5269  

3,4-DICHLORO-3',4',5'-TRIBB (13C12, 99%) 40 UG/ML IN NONANE

PCB-169  

3,3',4,4',5,5'-HEXACB UNLABELED 35 UG/ML IN ISOOCTANE